Evaporator circulation pump type CAHRM750K running at site (2020).
Evaporator circulation pump type CAHRM750K running at site (2020).

The challenge

The phosphoric acid is produced in a dihydrate (DH) process. The phosphate rock is attacked by phosphoric and sulfuric acid in a reactor. The 28%  P₂O₅ acid produced is filtrated and then evaporated to a concentration of 54% P₂O₅.

The constraints of the evaporator circulator are:

  • 54% P₂O₅ acid with contaminants (HF, H2SiF6, H2SO4,≈ 3% solids)
  • maximum operating temperature of 95°C
  • manufacturer standard design (high flow, low head and limited NPSHa)
  • no speed variation
  • heavy duty and nominal bearing duration > 25’000 hours of operation

The solution

Sulzer selected the best pump size and propeller design for optimum benefits to the customer:

  • propeller specifically designed for the project, with high efficiency and lasting performance in a corrosive and erosive application
  • optimal selection of the operating point with regard to the BEP and inherent hydraulic constraints of axial flow pump (high NS)
  • adapted mechanism for pulleys/belts assembly, guaranteeing perfect performance and long lifetime of the mechanical seals as well as trouble-free operation of the bearings

The material of construction proposed by the engineering company was SS904L, which is a common material for such applications. Its asset is a good corrosion resistance in most low-temperature P2O5 applications.

The Sulzer axial flow pump type CAHRM750K we use in the evaporator circulation loop as been running perfectly ever since the start-up and we are very satisfied. We only had to replace some parts after eight years of operation, which is remarkable.

Production Manager at NCIC

Customer benefit

An axial flow pump with a state-of-the-art design, adequately selected to meet exact production needs and properly serviced, proved to be highly beneficial to our customer.

The pump was operated for eight years without any repair. After that, the customer decided to replace the main wear parts: propeller, shaft, wear ring and mechanical seals. Although many of the parts could have been re-used, the customer chose to replace them with genuine new parts. Reusing worn components would not have guaranteed a similar lifetime after restart.

Despite an apparently low solids content in the fluid, the total weight of solids passing through the pump during one hour of operation can be estimated to be about 180 tons. These solids are mainly gypsum and precipitates. The traces of erosion visible on the propeller did not reveal abnormal patterns. The hydraulic design tailored for the project turned out to be successful and highly reliable.

During these eight years, the total cost of ownership (TCO) was kept to a minimum, with no added costs for commissioning, no down-time costs, no removal and disposal costs. The only costs were related to operation, i.e. energy and consumables, and routine maintenance.

Product specification
Chart of everlasting circulation pump

Project data

The pump is installed in an evaporation / concentration loop. It is located between the evaporator and the heat exchanger. It takes care of the continuous circulation of the phosphoric acid through the heat exchanger and the evaporator.

 

Application Evaporator circulation pump
Liquid 54% phosphoric acid @ 86°C
Pump type CAHRM750K
Material of construction Casing/wearing/shaft in WN 1.4539
Propeller in WN 1.4584
Nominal speed 520 (rpm)
Lubrication Grease
Installation Pump/motor side mounting on common baseplate
Motor SIEMENS 250 kW – 3’300 V - 50 Hz
Transmission Pulleys/belts (10 belts)
Mechanical seals John Crane P32+FA33

 

For further information on the selection and operation of axial flow pumps in an evaporation loop, consult the article Optimizing Axial Flow Pumps in Evaporator Circuit written by D. Krebs (43rd Annual International Phosphate Fertilizer & Sulfuric Acid Technology Conference, AIChE, Clearwater convention 2019) or read his article Optimizing the performance of axial flow pumps in evaporator circuits.

Product
  • CAHR axial flow pump
    The CAHR pump range has been designed for high flow and low head pumping applications. With its heavy-duty construction and flexible design, it is suitable for all kinds of industrial schemes and various types of liquids for both highly corrosive and slurry applications.
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